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Creators/Authors contains: "Weh, Dominik"

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  1. ; ; ; ; ; ; ; (, Inorganic Chemistry)
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  2. ; ; ; ; (, Zeitschrift für anorganische und allgemeine Chemie)
    Abstract p‐Fluorophenylisocyanide (CNPhpF) reacts with [Re(CO)5Br] under stepwise exchange of the carbonyl ligands depending on the conditions applied. The reaction stops with the formation offac‐[Re(CO)3Br(CNPhpF)2] in boiling THF. An ongoing carbonyl exchange is observed at higher temperatures, e. g. in refluxing toluene, with the final formation of the [Re(CNPhpF)6]+cation. The progress of the reactions has been studied by19F NMR spectroscopy and the structures of [Re(CO)Br(CNPhpF)4] and [Re(CNPhpF)6](BPh4) have been elucidated by X‐ray diffraction. 
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